1,6-二碘代十二氟己烷合成路线 （共 26 条）
反应条件
iodine T=225 - 245°C; P=27377.7 - 28952.9 Torr; 12 h;
参考文献
EP1422211 A1, ;
Page column 3 ;
反应条件
iodine in neat (no solvent) T=200 - 220°C; P=15200 - 20520 Torr; 22 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 45, # 2 p. 347 - 348
反应条件
iodine in neat (no solvent) T=200 - 220°C; P=15200 - 20520 Torr; 22 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 45, # 2 p. 347 - 348
反应条件
T=220°C; P=12901.3 Torr; 20 h;
参考文献
EP1422211 A1, ;
Page column 4 ;
反应条件
T=160 - 225°C; P=20702.1 - 25877.6 Torr; 22.5 h;
参考文献
EP1422211 A1, ;
Page column 5 ;
反应条件
iodine T=285°C; 8 h; var. TFE/iodine mol ratio; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 41, p. 293 - 296
反应条件
in neat (no solvent) T=200 - 220°C; 28 h;
参考文献
Bedford, Clifford D.; Baum, Kurt
Journal of Organic Chemistry, 1980 , vol. 45, # 2 p. 347 - 348
反应条件
potassium iodide T=270 - 375°C;
参考文献
Tetrahedron Letters, , p. 4761 - 4762
反应条件
1: Na2S2O4 / dimethylsulfoxide / 3 h / 20 °C 2: 54 percent / Na2S2O8; iodine / H2O; dimethylsulfoxide / 1 h / 20 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 128, # 10 p. 1187 - 1190
16486-97-81-氯-1,1,2,2,3,3,4,4,5,5,6,6-十二氟-6-碘己烷
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反应条件
1: Na2S2O4 / dimethylsulfoxide / 100 °C 2: 54 percent / Na2S2O8; iodine / H2O; dimethylsulfoxide / 1 h / 20 °C View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 128, # 10 p. 1187 - 1190
