(E)-2-甲基-2-丁烯酸苯甲酯合成路线 (共 18 条)
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane T=20°C; 0.166667 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 350, # 13 p. 2033 - 2038
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in toluene T=100°C; Mitsunobu reaction;
参考文献
Tetrahedron Letters, , vol. 44, # 18 p. 3609 - 3611
参考文献
Zhurnal Obshchei Khimii, , vol. 28, p. 503,503, 505; engl. Ausg. S. 494, 496
反应条件
1: [Ir(cod)Py(3)]+[BArF]-; hydrogen / dichloromethane / 1500.15 Torr / |Inert atmosphere 2: lithium aluminium tetrahydride / |Inert atmosphere View Scheme
参考文献
Li, Jia-Qi; Quan, Xu; Andersson, Pher G.
Chemistry - A European Journal, 2012 , vol. 18, # 34 p. 10609 - 10616
反应条件
1: With hydrogen; N-heterocyclic carbene complex in dichloromethane T=25°C; P=15201 Torr; 4 h; 2: With lithium aluminium tetrahydride Further stages. Title compound not separated from byproducts.;
参考文献
Zhou, Jianguang; Ogle, James W.; Fan, Yubo; Banphavichit, Yorawit; Zhu, Ye; Burgess, Kevin
Chemistry - A European Journal, 2007 , vol. 13, # 25 p. 7162 - 7170
反应条件
1: With hydrogen; N-heterocyclic carbene complex in dichloromethane T=25°C; P=15201 Torr; 4 h; 2: With lithium aluminium tetrahydride Further stages. Title compound not separated from byproducts.;
参考文献
Zhou, Jianguang; Ogle, James W.; Fan, Yubo; Banphavichit, Yorawit; Zhu, Ye; Burgess, Kevin
Chemistry - A European Journal, 2007 , vol. 13, # 25 p. 7162 - 7170
反应条件
1: hydrogen; [(D)*Ir(1,4-cyclooctadiene)]+[tetrakis(3,5-bis(trifluoromethyl)phenyl)borate]- / dichloromethane / 15 h / 20 °C / 15001.5 Torr / |Inert atmosphere 2: lithium aluminium tetrahydride / |Inert atmosphere View Scheme
参考文献
Li, Jia-Qi; Quan, Xu; Andersson, Pher G.
Chemistry - A European Journal, 2012 , vol. 18, # 34 p. 10609 - 10616
反应条件
[Ir(cod)Py(3)]+[BArF]-; hydrogen in dichloromethane
P=1500.15 Torr; Inert atmosphere;
参考文献
Li, Jia-Qi; Quan, Xu; Andersson, Pher G.
Chemistry - A European Journal, 2012 , vol. 18, # 34 p. 10609 - 10616