1: With hydrazine hydrate in methanol
1 h; Heating;
2: With hydrogenchloride in water
T=20°C; pH=4;
参考文献
Wang, Mingyao; McIntee, Edward J.; Shi, Yongli; Cheng, Guang; Upadhyaya, Pramod; Villalta, Peter W.; Hecht, Stephen S.
Chemical Research in Toxicology, 2001 , vol. 14, # 10 p. 1428 - 1434
1.1: 90 percent / 4-methylmorpholine N-oxide; OsO4 / tetrahydrofuran; H2O / 3 h / 20 °C
2.1: H2NNH2*H2O / methanol / 1 h / Heating
2.2: 75 percent / HCl / H2O / 20 °C / pH 4
View Scheme
参考文献
Wang, Mingyao; McIntee, Edward J.; Shi, Yongli; Cheng, Guang; Upadhyaya, Pramod; Villalta, Peter W.; Hecht, Stephen S.
Chemical Research in Toxicology, 2001 , vol. 14, # 10 p. 1428 - 1434
1.1: 77 percent / dimethylformamide / 6 h / 120 °C
2.1: 90 percent / 4-methylmorpholine N-oxide; OsO4 / tetrahydrofuran; H2O / 3 h / 20 °C
3.1: H2NNH2*H2O / methanol / 1 h / Heating
3.2: 75 percent / HCl / H2O / 20 °C / pH 4
View Scheme
参考文献
Wang, Mingyao; McIntee, Edward J.; Shi, Yongli; Cheng, Guang; Upadhyaya, Pramod; Villalta, Peter W.; Hecht, Stephen S.
Chemical Research in Toxicology, 2001 , vol. 14, # 10 p. 1428 - 1434
