1-(2-溴乙基)-3,5-二甲氧基苯合成路线 （共 13 条）
反应条件
1: diethyl ether
2: Ag2O
3: LiAlH4
4: CCl4; PBr3
View Scheme
参考文献
Carnmalm
Acta Chemica Scandinavica (1947-1973), 1955 , vol. 9, p. 246,249
反应条件
2: aqueous H2SO4
View Scheme
参考文献
Davies et al.
Journal of the Chemical Society, 1955 , p. 2782,2784
反应条件
1: 1) anhydrous sodium sulfite 2) dimethylformamide, thionyl chloride / 1) water, reflux, 24 h 2) benzene, reflux, 4 h
2: 78.7 percent / sodium azide / acetone; H2O / 12 h / Ambient temperature
3: 1.2 percent / 650 °C / 0 - 0.05 Torr
View Scheme
参考文献
Abramovitch, Rudolph A.; Holcomb, William D.; Thompson, W. Marshall; Wake, Shigeo
Journal of Organic Chemistry, 1984 , vol. 49, # 26 p. 5124 - 5131
