甲基2-氨基-3-氧代四氢-1H-吡咯里嗪-7A(5H)-羧酸酯合成路线 （共 2 条）
反应条件
hydrogen; palladium dihydroxide in methanol
T=20°C; P=26600 Torr; 20 h;
参考文献
Cordero, Franca M.; Pisaneschi, Federica; Batista, Karina Meschini; Valenza, Silvia; Machetti, Fabrizio; Brandi, Alberto
Journal of Organic Chemistry, 2005 , vol. 70, # 3 p. 856 - 867
反应条件
1: 42 percent / H2O / 14 h / 60 °C
2: 96 percent / acetic acid; H2 / Pd(OH)2/C / methanol / 12 h / 20 °C / atmospheric pressure
3: pyridine / CH2Cl2 / 0.5 h / 0 °C
4: CH2Cl2 / 0.5 h / 0 °C
5: H2 / Pd(OH)2/C / methanol / 20 h / 20 °C / 26600 Torr
View Scheme
参考文献
Cordero, Franca M.; Pisaneschi, Federica; Batista, Karina Meschini; Valenza, Silvia; Machetti, Fabrizio; Brandi, Alberto
Journal of Organic Chemistry, 2005 , vol. 70, # 3 p. 856 - 867
