N-苯基双(三氟甲烷磺酰)亚胺合成路线 （共 107 条）
反应条件
triethylamine in dichloromethane T=25°C; 16 h; Inert atmosphereIndustry scaleCooling with ice;
参考文献
US2012/316204 A1, ;
Page/Page column 7-8 ;
反应条件
triethylamine in dichloromethane T=-78 - 20°C; Inert atmosphere;
参考文献
US2011/230495 A1, ;
Page/Page column 17 ;
参考文献
Zhurnal Organicheskoi Khimii, , vol. 10, p. 901 - 902
Zhurnal Organicheskoi Khimii, , vol. 10, p. 889 - 890
C.A., , vol. 81, p. 25298
反应条件
in freon 113=1,1,2-trichloro-trifluoroethane at 95°C;
参考文献
Zhurnal Organicheskoi Khimii, , vol. 8, p. 1696 - 1699
Zhurnal Organicheskoi Khimii, , vol. 8, p. 1659 - 1662
参考文献
Journal of Organic Chemistry, , vol. 72, # 18 p. 6758 - 6762
反应条件
[Bmim][Br] T=24.84°C; 24 h; Kinetics;
参考文献
Chemical Communications, , # 8 p. 897 - 899
反应条件
potassium carbonate in tetrahydrofuran T=120°C; 0.1 h; Microwave irradiation;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 21, # 1 p. 137 - 140
反应条件
sodium hydride Multistep reaction;
参考文献
Houpis, Ioannis N.
Tetrahedron Letters, 1991 , vol. 32, # 46 p. 6675 - 6678
反应条件
1: 4-morpholin-4-yl-cyclohexanone With lithium hexamethyldisilazane in tetrahydrofuran T=-78°C; 1 h; 2: N,N-bis(trifluoromethanesulfonyl)aniline in tetrahydrofuran T=-78 - 20°C; 20.5 h;
参考文献
EISAI R andamp; D MANAGEMENT CO. LTD; GRACZYK, Piotr; BHATIA, Gurpreet, Singh
Patent: WO2010/15803 A1, 2010 ;
Location in patent: Page/Page column 32; 35 ;
WO 2010/015803 A1
参考文献
Hendrickson,J.B.; Bergeron,R.
Tetrahedron Letters, 1973 , # 46 p. 4607 - 4610
