2,2,3,3,3,4,4,5,5-八氟戊酸合成路线 (共 18 条)
反应条件
sodium hypochlorite; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; potassium bromide in acetonitrile T=20°C; pH=8 - 9; 48 h; Product distribution / selectivity;
参考文献
Ignatowska, Jolanta; Shyshkov, Oleg; Zipplies, Tilman; Hintzer, Klaus; Roeschenthaler, Gerd-Volker
Journal of Fluorine Chemistry, 2012 , vol. 141, p. 35 - 40
参考文献
Journal of the Chemical Society, , p. 3035 - 3043
参考文献
Journal of Organic Chemistry, , vol. 25, p. 180 - 182
参考文献
Industrial and Engineering Chemistry, , vol. 39, p. 415,416
反应条件
sodium hydroxide 2.) ethylene glycol, 180 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Matsuo, Keizo; Stockmayer, Walter H.
Journal of Physical Chemistry, 1981 , vol. 85, # 22 p. 3307 - 3311
参考文献
Levin,A.I. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, # 10 p. 1778 - 1781,1776 - 1778
反应条件
benzoyl chloride Heating;
参考文献
Chengxue, Zhao; Renmo, Zhou; Heqi, Pan; Xiangshan, Jin; Yangling, Qu; et al.
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2009 - 2013
反应条件
sodium carbonate in tetrahydrofuran T=66°C; 10 h;
参考文献
Yoshino, Norio; Komine, Noboru; Suzuki, Jun-ichi; Arima, Yuki; Hirai, Hidefumi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 11 p. 3262 - 3266
参考文献
McBee; Wiseman; Bachman
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 415,416
反应条件
lithium aluminium tetrahydride
参考文献
Matsuo, Keizo; Stockmayer, Walter H.
Journal of Physical Chemistry, 1981 , vol. 85, # 22 p. 3307 - 3311