2,2,3,3,3,4,4,5,5-八氟戊酸合成路线 (共 18 条)
反应条件
(chlorodifluoromethyl)benzene; diboron trioxide; titanium tetrachloride T=60 - 100°C;
参考文献
Schwertfeger, W.; Siegemund, G.
Journal of Fluorine Chemistry, 1987 , vol. 36, p. 237 - 246
反应条件
1: pyridine; thionyl chloride 2: water; ammonia View Scheme
参考文献
Du Pont de Nemours and Co.
Patent: US2646449 , 1950 ;
反应条件
lithium aluminium tetrahydride
参考文献
Matsuo, Keizo; Stockmayer, Walter H.
Journal of Physical Chemistry, 1981 , vol. 85, # 22 p. 3307 - 3311
参考文献
Harris,J.F.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2182 - 2190
反应条件
1: pyridine; thionyl chloride
2: water; ammonia
3: lithium alanate; diethyl ether
View Scheme
参考文献
Du Pont de Nemours and Co.
Patent: US2646449 , 1950 ;
反应条件
1: LiAlH4
2: SF4 / 48 h / 150 °C
View Scheme
参考文献
Matsuo, Keizo; Stockmayer, Walter H.
Journal of Physical Chemistry, 1981 , vol. 85, # 22 p. 3307 - 3311
反应条件
1: COF2, NaF
2: KF*HF / acetonitrile / 9 h / 100 - 125 °C
View Scheme
参考文献
Smith,R.D. et al.
Journal of the American Chemical Society, 1962 , vol. 84, p. 4285 - 4288
反应条件
chlorine
Irradiation;
参考文献
Zapevalov,A.Ya. et al.
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, p. 259 - 262,239 - 242