1,1,2,2,3,3,4,4,5,5-十氟环戊烷合成路线 (共 22 条)
反应条件
hydrogen fluoride
T=5 - 6°C; 7 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.2 - 8.1 V; Further byproducts given. Yields of byproduct given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 7.45 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.5 - 9.0 V; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 7.45 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.5 - 9.0 V; Further byproducts given. Yields of byproduct given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 7.45 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.5 - 9.0 V; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 4.68333 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.1 - 8.1 V; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=5 - 6°C; 4.68333 h; electrochemical fluorination; anodic current density 3.5 A/dm2, 5.1 - 8.1 V; Further byproducts given. Yields of byproduct given;
参考文献
Abe,T.; Baba,H.; Hayashi,E.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 123
反应条件
hydrogen fluoride
T=7 - 8°C; 6.15 h; Electrochemical reaction;
参考文献
Abe, Takashi; Tamura, Masanori; Sekiya, Akira
Journal of Fluorine Chemistry, 2005 , vol. 126, # 3 p. 325 - 332
反应条件
fluorine
T=-30 - 10°C; Irradiationsteady-state flow process; the hydrocarbon vapor is condensed onto a NaF preaerosol and then subjected to attack by an excess of elemental F in He at first in the dark, then under UV irradiation; MechanismProduct distribution;
参考文献
Adcock, James L.; Evans, William D.
Journal of Organic Chemistry, 1984 , vol. 49, # 15 p. 2719 - 2723
反应条件
on fluorination of perfluorcyclopentene with hexafluoride at 50 up to 70°C in a period of 48 hours; a scarce amt. of Xe was formed;;
参考文献
Gard, G. L.; Cady, G. H.
Inorganic Chemistry, 1964 , vol. 3, p. 1745 - 1745
参考文献
Barber et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 4241