甲基 2,3-二-O-二苯基膦基-4,6-O-亚苄基吡喃葡萄糖苷合成路线 (共 3 条)
反应条件
1: 2-methyl-but-3-yn-2-ol With triethylamine in dichloromethane
T=-85°C; 0.166667 h;
2: benzenesulfenyl chloride in dichloromethane
T=-85 - 20°C;
参考文献
Ma, Shengming; Ren, Hongjun; Wei, Qi
Journal of the American Chemical Society, 2003 , vol. 125, # 16 p. 4817 - 4830
反应条件
lithium aluminium tetrahydride
参考文献
Cookson,R.C.; Parsons,P.J.
Journal of the Chemical Society, Chemical Communications, 1978 , p. 822 - 824
反应条件
pyridine; tetraphosphorus decasulfide in dichloromethane
T=20°C; 5.5 h;
参考文献
Ma, Shengming; Hao, Xueshi; Meng, Xiaofeng; Huang, Xian
Journal of Organic Chemistry, 2004 , vol. 69, # 17 p. 5720 - 5724