反应条件
in tetrahydrofuran
(N2), Schlenk techniques; addn. of Ge compd. to soln. of Mg compd. in C4H8O at 0°C, stirring at room temp. for 12 h; addn. of satd. aq. NH4Cl, extn. with Et2O, washing with satd. NaCl, drying (MgSO4), evapn., distillation (30 mm Hg, 110°C);
参考文献
Hasegawa, Munehiro; Usui, Ippei; Konno, Soichiro; Murakami, Masahiro
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4169 - 4175
