1: 55 percent / 60percent H2SO4 / 2.5 h / 130 °C
2: 70 percent / polyphosphoric acid / 2.5 h / 100 °C
3: 22.5 g / 15percent methanolic HCl / 30 h / Ambient temperature
4: 9.62 g / NaBH4 / methanol / 2 h / Ambient temperature
5: 9.8 g / pyridine
6: 7.8 g / NaOH/85percent aq. MeOH / 2.5 h / Heating
7: 6.2 g / Jones' reagent / acetone / 0.5 h / 0 - 5 °C
8: 0.18 g / diethyl ether
View Scheme
参考文献
Thakur, S. B.; Jadhav, K. S.; Bhattacharyya, S. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 675 - 683
1: 40 g / 10percent aq. NaOH / 4 h / Heating
2: 55 percent / 60percent H2SO4 / 2.5 h / 130 °C
3: 70 percent / polyphosphoric acid / 2.5 h / 100 °C
4: 22.5 g / 15percent methanolic HCl / 30 h / Ambient temperature
5: 9.62 g / NaBH4 / methanol / 2 h / Ambient temperature
6: 9.8 g / pyridine
7: 7.8 g / NaOH/85percent aq. MeOH / 2.5 h / Heating
8: 6.2 g / Jones' reagent / acetone / 0.5 h / 0 - 5 °C
9: 0.18 g / diethyl ether
View Scheme
参考文献
Thakur, S. B.; Jadhav, K. S.; Bhattacharyya, S. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 675 - 683
1: 30percent aq.H2SO4 / aq. acetic acid / 16 h / Heating
2: 58 g / p-toluenesulfonic acid / benzene / 6 h / Heating
View Scheme
参考文献
Lapitskaya, M. A.; Manukina, T. A.; Nozdracheva, A. T.; Sheimina, L. G.; Pivnitskii, K. K.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 261 - 265
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 2 p. 294 - 299
1: 9.62 g / NaBH4 / methanol / 2 h / Ambient temperature
2: 9.8 g / pyridine
3: 7.8 g / NaOH/85percent aq. MeOH / 2.5 h / Heating
4: 6.2 g / Jones' reagent / acetone / 0.5 h / 0 - 5 °C
5: 0.18 g / diethyl ether
View Scheme
参考文献
Thakur, S. B.; Jadhav, K. S.; Bhattacharyya, S. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 675 - 683
1: 9.8 g / pyridine
2: 7.8 g / NaOH/85percent aq. MeOH / 2.5 h / Heating
3: 6.2 g / Jones' reagent / acetone / 0.5 h / 0 - 5 °C
4: 0.18 g / diethyl ether
View Scheme
参考文献
Thakur, S. B.; Jadhav, K. S.; Bhattacharyya, S. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 675 - 683
1: 6.2 g / Jones' reagent / acetone / 0.5 h / 0 - 5 °C
2: 0.18 g / diethyl ether
View Scheme
参考文献
Thakur, S. B.; Jadhav, K. S.; Bhattacharyya, S. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 675 - 683
1: 7.8 g / NaOH/85percent aq. MeOH / 2.5 h / Heating
2: 6.2 g / Jones' reagent / acetone / 0.5 h / 0 - 5 °C
3: 0.18 g / diethyl ether
View Scheme
参考文献
Thakur, S. B.; Jadhav, K. S.; Bhattacharyya, S. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 675 - 683
