[(Z)-2-甲基磺酰基乙烯基]苯合成路线 （共 14 条）
反应条件
4 A molecular sieve; magnesium; triethyl phosphite; bis(cyclopentadienyl)titanium dichloride in tetrahydrofuran T=0°C; 13 h;
参考文献
Ogata, Akitoshi; Nemoto, Masami; Kobayashi, Kenji; Tsubouchi, Akira; Takeda, Takeshi
Journal of Organic Chemistry, 2007 , vol. 72, # 10 p. 3816 - 3822
反应条件
silver nitrate in tetrahydrofuran; water
T=20°C; 36 h; Inert atmosphere;
参考文献
Deng, Gui Sheng; Sun, Teng Fei
Chinese Chemical Letters, 2012 , vol. 23, # 10 p. 1115 - 1118,4
反应条件
dihydrogen peroxide; acetic acid
参考文献
Truce; Simms
Journal of the American Chemical Society, 1956 , vol. 78, p. 2756,2758
反应条件
1: sodium methanethiolate; ethanol
2: aqueous H2O2; acetic acid
View Scheme
参考文献
Truce; Simms
Journal of the American Chemical Society, 1956 , vol. 78, p. 2756,2758
反应条件
cesium fluoride in dimethyl sulfoxide
T=40°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bonini, Bianca Flavia; Comes-Franchini, Mauro; Fochi, Mariafrancesca; Mazzanti, Germana; Peri, Francesca; Ricci, Alfredo
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 23 p. 2803 - 2809
反应条件
1: 95 percent / HCl, H2S / diethyl ether / -30 °C
2: 98 percent / K2CO3 / acetone / Ambient temperature
3: 98 percent / aq. oxone / methanol / 4 h / Ambient temperature
4: aq. CsF / dimethylsulfoxide / 40 °C
View Scheme
参考文献
Bonini, Bianca Flavia; Comes-Franchini, Mauro; Fochi, Mariafrancesca; Mazzanti, Germana; Peri, Francesca; Ricci, Alfredo
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 23 p. 2803 - 2809
反应条件
1: 98 percent / K2CO3 / acetone / Ambient temperature
2: 98 percent / aq. oxone / methanol / 4 h / Ambient temperature
3: aq. CsF / dimethylsulfoxide / 40 °C
View Scheme
参考文献
Bonini, Bianca Flavia; Comes-Franchini, Mauro; Fochi, Mariafrancesca; Mazzanti, Germana; Peri, Francesca; Ricci, Alfredo
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 23 p. 2803 - 2809
反应条件
1: 98 percent / aq. oxone / methanol / 4 h / Ambient temperature
2: aq. CsF / dimethylsulfoxide / 40 °C
View Scheme
参考文献
Bonini, Bianca Flavia; Comes-Franchini, Mauro; Fochi, Mariafrancesca; Mazzanti, Germana; Peri, Francesca; Ricci, Alfredo
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 23 p. 2803 - 2809
反应条件
acetophenone in benzene
T=25°C; Irradiationsensitized photoisomerization; different reaction times;
参考文献
Wegener, Wolfgang; Hoffmann, Katrin; Alder, Lutz; Michael, Guenter; Schleinitz, Klaus-Dieter
Zeitschrift fuer Chemie (Stuttgart, Germany), 1981 , vol. 21, # 4 p. 151
反应条件
1: diisobutylaluminium hydride
2: potassium peroxymonosulfate
View Scheme
参考文献
Oishi, Shigeki; Hatano, Keisuke; Tsubouchi, Akira; Takeda, Takeshi
Chemical Communications, 2011 , vol. 47, # 42 p. 11639 - 11640
