1,1,1-三甲基-N-苯基哌啶合成路线 （共 76 条）
反应条件
diphenylether; pentacarbonyliron(0) in tetrahydrofuran T=100°C; 2 h; Yield given;
参考文献
Saidi, Mohammad R; Azizi, Najmoddin; Zali-Boinee, Hasan
Tetrahedron, 2001 , vol. 57, # 31 p. 6829 - 6832
反应条件
triethylamine in diethyl ether 8 h; Heating;
参考文献
Mizhiritskii, M. D.; Reikhsfel'd, V. O.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 7 p. 1547 - 1558,1373 - 1382
反应条件
sodium methylate in tetrahydrofuran; diethylene glycol dimethyl ether T=40°C; 18 h;
参考文献
Ando, Wataru; Tsumaki, Hidetoshi
Chemistry Letters, 1981 , p. 693 - 694
反应条件
sodium methylate in tetrahydrofuran; diethylene glycol dimethyl ether 20 h; Ambient temperature;
参考文献
Ando, Wataru; Tsumaki, Hidetoshi
Chemistry Letters, 1981 , p. 693 - 694
反应条件
nitrosyl chloride in dichloromethane 0.166667 h; Ambient temperature;
参考文献
Weiss, Robert; Wagner, Klaus-Georg; Hertel, Marion
Chemische Berichte, 1984 , vol. 117, # 5 p. 1965 - 1972
反应条件
NOBF4 in dichloromethane Ambient temperature;
参考文献
Weiss, Robert; Wagner, Klaus-Georg; Hertel, Marion
Chemische Berichte, 1984 , vol. 117, # 5 p. 1965 - 1972
反应条件
nitrosyl bromide in dichloromethane 0.166667 h; Ambient temperature;
参考文献
Weiss, Robert; Wagner, Klaus-Georg; Hertel, Marion
Chemische Berichte, 1984 , vol. 117, # 5 p. 1965 - 1972
反应条件
in dichloromethane Ambient temperature;
参考文献
Weiss, Robert; Wagner, Klaus-Georg; Hertel, Marion
Chemische Berichte, 1984 , vol. 117, # 5 p. 1965 - 1972
反应条件
acetic acid 1) CH2Cl2, (-10)-(-15) deg C, 2 h; reflux, 3 h; 2) (-10)-(-15) deg C, 3 h; Multistep reaction. Further byproducts given;
参考文献
Kanetani, Fujio; Okada, Eiji; Negoro, Kenji
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 8 p. 2517 - 2520
反应条件
cesium fluoride; bis(dibenzylideneacetone)-palladium(0); 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl T=100°C; 5.5 h; Inert atmosphere;
参考文献
Shimizu, Kenta; Minami, Yasunori; Goto, Osamu; Ikehira, Hideyuki; Hiyama, Tamejiro
Chemistry Letters, 2014 , vol. 43, # 4 p. 438 - 440
