1,1,2,2,3,3,4,4-八氟丁烷合成路线 (共 19 条)
反应条件
sodium hydroxide Heating;
参考文献
Ward,R.B.
Journal of Organic Chemistry, 1965 , vol. 30, p. 3009 - 3011
反应条件
in 1,2,2-trifluoro-trichloroethane 48 h; Ambient temperature;
参考文献
Chengxue, Zhao; Renmo, Zhou; Heqi, Pan; Xiangshan, Jin; Yangling, Qu; et al.
Journal of Organic Chemistry, 1982 , vol. 47, # 11 p. 2009 - 2013
反应条件
in diethyl ether; ammonia T=0°C;
参考文献
Saloutina, L. V.; Zapevalov, A. Ya.; Kolenko, I. P.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 11 p. 2019 - 2024
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 11 p. 2250 - 2256
反应条件
cobalt(III) fluoride T=140 - 230°C; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Burdon, James; Ezmirly, Saleh T.; Huckerby, Thomas N.
Journal of Fluorine Chemistry, 1988 , vol. 40, p. 283 - 318
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1) 15 min, 0 deg C 2) 20h, 10 deg C; Yield given. Yields of byproduct given;
参考文献
Chen, Quing-Yun; Chen, Ming-Fang
Journal of Fluorine Chemistry, 1990 , vol. 49, # 1 p. 107 - 114
反应条件
in ethylene glycol 5 h; Heating; Yield given;
参考文献
Hudlicky, Tomas; Fan, Rulin; Reed, Josephine W.; Carver, David R.; Hudlicky, Milos; Eger, Edmond I.
Journal of Fluorine Chemistry, 1992 , vol. 59, # 1 p. 9 - 14
参考文献
Haszeldine; Marklow
Journal of the Chemical Society, 1956 , p. 962,968
反应条件
sodium hydroxide 2.) ethylene glycol, 180 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Matsuo, Keizo; Stockmayer, Walter H.
Journal of Physical Chemistry, 1981 , vol. 85, # 22 p. 3307 - 3311
反应条件
sodium hydroxide; sulfuric acid 1.) H2O, reflux, 30 min, 2.) reflux; Product distribution;
参考文献
Saloutina, L. V.; Zapevalov, A. Ya.; Kodess, M. I.; Kolenko, I. P.; German, L. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1023 - 1025
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 5 p. 1114 - 1116