Z-PHE-GLY-GLY-OH合成路线 （共 10 条）
反应条件
hydrogen; palladium on activated charcoal in methanol 5 h;
参考文献
Ovchinnikov, Mikhail V.; Bespalova, Zhanna D.; Molokoedov, Aleksandr S.; Revenko, Inna V.; Sepetov, Nikolai F.; et al
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 3 p. 784 - 795
反应条件
triethylamine in water; acetonitrile
T=20°C;
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.
Synthesis, 2004 , # 16 p. 2645 - 2652
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1: 70 percent / NEt3 / CH2Cl2 / 4 h / 0 °C
2: Jones' reagent / acetone / 3 h / 0 °C
3: 99 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
4: 99 percent / Jones' reagent
5: 35 percent / DCC
6: 80 percent / Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1: Jones' reagent / acetone / 3 h / 0 °C
2: 99 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
3: 99 percent / Jones' reagent
4: 35 percent / DCC
5: 80 percent / Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1: 70 percent / NEt3 / CH2Cl2 / 4 h / 0 °C
2: Jones' reagent / acetone / 3 h / 0 °C
3: 99 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
4: 99 percent / Jones' reagent
5: 35 percent / DCC
6: 80 percent / Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
1.1: SOCl2 / tetrahydrofuran / 0.33 h / 25 °C
1.2: 89 percent / tetrahydrofuran / 1 h / 25 °C
2.1: 98 percent / Et3N / acetonitrile; H2O / 20 °C
View Scheme
参考文献
Katritzky, Alan R.; Suzuki, Kazuyuki; Singh, Sandeep K.
Synthesis, 2004 , # 16 p. 2645 - 2652
反应条件
1: aq. NaOH/aq. H2O2 / ethanol / 0.33 h / 65 °C
2: 99 percent / DCC / CH2Cl2 / 10 h / Ambient temperature
3: 99 percent / Jones' reagent
4: 35 percent / DCC
5: 80 percent / Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
反应条件
in N,N-dimethyl-formamide
T=20°C; 15 h; Yield given;
参考文献
Ovchinnikov, Mikhail V.; Bespalova, Zhanna D.; Molokoedov, Aleksandr S.; Revenko, Inna V.; Sepetov, Nikolai F.; et al
Collection of Czechoslovak Chemical Communications, 1989 , vol. 54, # 3 p. 784 - 795
反应条件
1: 35 percent / DCC
2: 80 percent / Jones' reagent
View Scheme
参考文献
Kashima, Choji; Harada, Kazuo; Fujioka, Yoko; Maruyama, Tatsuya; Omote, Yoshimori
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 535 - 540
