反应条件
1: 97 percent / pyridine / 1 h / 20 °C
2: 83 percent / 3 percent HCl in MeOH / diethyl ether / 20 °C
3: periodinane / CH2Cl2 / 2 h / 20 °C
4: 75 percent / NaN(SiMe3)2 / tetrahydrofuran / 0.5 h / 20 °C
5: 85 percent / (S)-BINAL-H / 2 h / -100 °C
6: 1N aq. NaOH / tetrahydrofuran; methanol / 1 h / 20 °C
View Scheme
参考文献
Durand, Thierry; Cracowski, Jean-Luc; Guy, Alexandre; Rossi, Jean-Claude
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 18 p. 2495 - 2498
