5-亚甲基螺[2.4]庚烷合成路线 (共 27 条)
反应条件
tri-iso-propyl phosphine; bis(dibenzylideneacetone)-palladium(0) in benzene
T=100°C; 4 h;
参考文献
Binger, Paul; Schuchardt, Ulf
Chemische Berichte, 1980 , vol. 113, # 10 p. 3334 - 3341
反应条件
monoethoxy-diethylaluminum; tri-iso-propyl phosphine; bis(acetylacetonato) palladium in toluene
T=100°C; 16 h;
参考文献
Binger, Paul; Schuchardt, Ulf
Chemische Berichte, 1981 , vol. 114, # 10 p. 3313 - 3324
反应条件
3-methyl-1,2-butadiene; palladium(II) 2,4-pentanedionate; monoethoxy-diethylaluminum; tri-iso-propyl phosphine in benzene
T=100°C; 4 h;
参考文献
Binger, Paul; Schuchardt, Ulf
Chemische Berichte, 1980 , vol. 113, # 3 p. 1063 - 1071
反应条件
methylene cyclopropane; tri-iso-propyl phosphine; bis(dibenzylideneacetone)-palladium(0) in benzene
T=115°C; 20 h;
参考文献
Binger, Paul; Schuchardt, Ulf
Chemische Berichte, 1980 , vol. 113, # 10 p. 3334 - 3341
反应条件
bis(dibenzylideneacetone)-palladium(0); tri-iso-propyl phosphine in benzene
T=100°C; 4 h;
参考文献
Binger, Paul; Schuchardt, Ulf
Chemische Berichte, 1980 , vol. 113, # 3 p. 1063 - 1071
反应条件
tri-iso-propyl phosphine; bis(dibenzylideneacetone)-palladium(0) in benzene
T=100°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Binger, Paul; Schuchardt, Ulf
Chemische Berichte, 1980 , vol. 113, # 10 p. 3334 - 3341
反应条件
tri-iso-propyl phosphine; (η3-allyl)(η5-Cp)Pd in toluene
T=130°C; 2.5 h; in dependence on catalyst, time, temperature; Product distribution;
参考文献
Binger, Paul; Schuchardt, Ulf
Chemische Berichte, 1981 , vol. 114, # 10 p. 3313 - 3324
反应条件
palladium(II) 2,4-pentanedionate; monoethoxy-diethylaluminum; tri-iso-propyl phosphine in benzene
T=100°C; 2 h;
参考文献
Binger, Paul; Schuchardt, Ulf
Chemische Berichte, 1980 , vol. 113, # 3 p. 1063 - 1071
反应条件
triphenyl phosphite; bis(1,5-cyclooctadiene)nickel (0) in toluene
T=20°C;
参考文献
Thormeier, Sabine; Carboni, Bertrand; Kaufmann, Dieter E
Journal of Organometallic Chemistry, 2002 , vol. 657, # 1-2 p. 136 - 145
反应条件
bis(1,5-cyclooctadiene)nickel (0)
T=35°C; 20 h;
参考文献
Binger, Paul; Brinkmann, Axel; Wedemann,Petra
Chemische Berichte, 1983 , vol. 116, # 8 p. 2920 - 2930