2-亚甲基丙烷-1,3-二基二乙酸酯合成路线 （共 21 条）
反应条件
hydrogenchloride in ethanol Heating;
参考文献
Chalova, O. B.; Chistoedova, G. B.; Kiladze, T. K.; Germash, E. V.; Kantor, E. A.; Rakhmankulov, D. L.
J. Appl. Chem. USSR (Engl. Transl.), 1988 , vol. 61, # 4 p. 934 - 937,853 - 855
反应条件
sodium methylate; nickel monoaluminide in methanol
参考文献
Bayer Aktiengesellschaft
Patent: US4036895 A1, 1977 ;
反应条件
sodium hydroxide; acetic acid; nickel monoaluminide in methanol; methyl acetate; water
参考文献
Bayer Aktiengesellschaft
Patent: US4036895 A1, 1977 ;
反应条件
sodium methylate in methanol
参考文献
Bayer Aktiengesellschaft
Patent: US4036895 A1, 1977 ;
反应条件
hydrogen; sodium methylate; acetic acid in methanol; methyl acetate; water
参考文献
Bayer Aktiengesellschaft
Patent: US4036895 A1, 1977 ;
反应条件
Candida antarctica lipase B in dichloromethane
T=20°C; 24 h; Enzymatic reaction;
参考文献
Sari, Ozkan; Hamada, Manabu; Roy, Vincent; Nolan, Steven P.; Agrofoglio, Luigi A.
Organic Letters, 2013 , vol. 15, # 17 p. 4390 - 4393
反应条件
1: Methyltriphenylphosphonium bromide With lithium hexamethyldisilazane in tetrahydrofuran
T=0°C; 1 h;
2: 1,3-Diacetoxy-acetone in tetrahydrofuran
T=-78°C; 3 h;
参考文献
Sari, Ozkan; Hamada, Manabu; Roy, Vincent; Nolan, Steven P.; Agrofoglio, Luigi A.
Organic Letters, 2013 , vol. 15, # 17 p. 4390 - 4393
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane
T=25°C; 24 h;
参考文献
Damez; Labrosse; Lhoste; Sinou
Synthesis, 2001 , # 10 p. 1456 - 1458
反应条件
18-crown-6 ether in N,N-dimethyl-formamide
T=100°C; 1 h;
参考文献
Friedrich, Marko; Savchenko, Andrei I.; Waechtler, Andreas; De Meijere, Armin
European Journal of Organic Chemistry, 2003 , # 11 p. 2138 - 2143
反应条件
in N,N-dimethyl-formamide
T=150°C; 1 h;
参考文献
Chalova, O. B.; Chistoedova, G. B.; Kiladze, T. K.; Germash, E. V.; Kantor, E. A.; Rakhmankulov, D. L.
J. Appl. Chem. USSR (Engl. Transl.), 1988 , vol. 61, # 4 p. 934 - 937,853 - 855
