反应条件
1: 1.) POCl3, 2.) Ag2O / 1.) dichloroethane, 0 deg C, 1 h; 25 deg C, 2.) water, 25 deg C, 60 h
2: LiOH, LiCl / H2O / 6 h / 25 °C / electrolysis: the cathode - mercury pool, the anode - platinum grid
3: diethyl ether
4: 55 percent / LiAlH4 / diethyl ether
5: 70 percent / Et3N / CH2Cl2
6: n-BuNClO4 / dimethylformamide / 6 h / 5 °C / electrolysis: Pb plate cathode, Pt grid anode
View Scheme
参考文献
Konstantinova, T. G.; Moiseenkov, A. M.; Shostakovskii, V. M.; Gul'tyai, V. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 4 p. 812 - 815
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 4 p. 893 - 896
