2,3,5-三-苄基-D-阿拉伯呋喃糖苷合成路线 (共 4 条)
反应条件
1: 44 g / pyridine / CH2Cl2 / Ambient temperature 2: hydrogen chloride / CH2Cl2 / 0.17 h / 0 °C 3: 3.5 g / triethylamine / acetonitrile / 1.25 h 4: 1.8 g / phosphoryl chloride, triethylamine / CHCl3 / 2 h / Heating 5: 0.2 g / boron trichloride / CH2Cl2 / 2 h / Ambient temperature 6: 68 percent / ammonia / ethanol / 6 h / 150 °C View Scheme
参考文献
Kadir, Kamaliah; Mackenzie, Grahame; Shaw, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2304 - 2309
反应条件
pyridine in dichloromethane Ambient temperature;
参考文献
Kadir, Kamaliah; Mackenzie, Grahame; Shaw, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2304 - 2309
参考文献
Franks,N.E.; Montgomery,R.
Carbohydrate Research, 1967 , vol. 3, p. 511 - 512
反应条件
1: 44 g / pyridine / CH2Cl2 / Ambient temperature
2: hydrogen chloride / CH2Cl2 / 0.17 h / 0 °C
View Scheme
参考文献
Kadir, Kamaliah; Mackenzie, Grahame; Shaw, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2304 - 2309