(S)-2-苯基-1-丙醇合成路线 （共 88 条）
反应条件
dichlorobis(1-neomenthylindenyl)zirconium; oxygen 1.) 1,2-dichloroethane, 22 deg C, 528 h, 2.) 1,2-dichloroethane, 0 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Petros, Robby A.; Camara, James M.; Norton, Jack R.
Journal of Organometallic Chemistry, 2007 , vol. 692, # 21 p. 4768 - 4773
反应条件
porcine pancreatic lipase in various solvent(s) 0.5 h; Title compound not separated from byproducts;
参考文献
Serra, Stefano
Tetrahedron Asymmetry, 2011 , vol. 22, # 6 p. 619 - 628
反应条件
1: With N-undecane; hydrogen; [rhodium(I)(carbonyl)2(acetylacetonate)]; triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt T=45°C; P=37503.8 Torr; 6 h; 2: With lithium aluminium tetrahydride in tetrahydrofuran Further stages. Title compound not separated from byproducts.;
参考文献
Leclercq, Loic; Suisse, Isabelle; Agbossou-Niedercorn, Francine
Chemical Communications, 2008 , # 3 p. 311 - 313
反应条件
baker's yeast; [14C]-Sucrose in ethanol T=30°C; 48 h;
参考文献
Ferraboschi, Patrizia; Reza-Elahi, Shahrzad; Verza, Elisa; Santaniello, Enzo
Tetrahedron Asymmetry, 1999 , vol. 10, # 14 p. 2639 - 2642
反应条件
1: With ozone in hexane; chloroform T=-78°C; ozonolysis; 2: With zinc in hexane; chloroform T=-78 - 0°C; Reduction; 0.166667 h; 3: With diisobutylaluminium hydride in hexane; chloroform; toluene T=-78 - 20°C; Reduction;
参考文献
Toda, Ayako; Aoyama, Hiroshi; Mimura, Norio; Ohno, Hiroaki; Fujii, Nobutaka; Ibuka, Toshiro
Journal of Organic Chemistry, 1998 , vol. 63, # 20 p. 7053 - 7061
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C;
参考文献
Schaefer, Carsten; Fu, Gregory C.
Angewandte Chemie - International Edition, 2005 , vol. 44, # 29 p. 4606 - 4608
反应条件
1: With ozone in acetone T=-78°C; 2: With sodium tetrahydroborate T=-78 - 20°C;
参考文献
Ohmiya, Hirohisa; Makida, Yusuke; Li, Dong; Tanabe, Masahito; Sawamura, Masaya
Journal of the American Chemical Society, 2010 , vol. 132, # 2 p. 879 - 889
反应条件
palladium 10 on activated carbon; hydrogen in methanol
参考文献
Serra, Stefano
Tetrahedron Asymmetry, 2011 , vol. 22, # 6 p. 619 - 628
反应条件
samarium diiodide; water; triethylamine in tetrahydrofuran T=20°C; 2 h; Inert atmosphereSchlenk technique; Reagent/catalyst;
参考文献
Szostak, Michal; Spain, Malcolm; Procter, David J.
Chemistry - A European Journal, 2014 , vol. 20, # 15 p. 4222 - 4226
反应条件
1: RhCl(PPh3)3 / benzene / 24 h / Ambient temperature 2: 30percent KOH / methanol; H2O / 0.17 h View Scheme
参考文献
Maslinska-Solich, Jolanta; Rudnicka, Irena; Jedlinski, Zbigniew J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3034 - 3040
