2-溴乙基基苯硼酸频哪醇酯合成路线 （共 25 条）
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in acetonitrile T=90°C; 2 h;
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 48 h / 85 °C / |Inert atmosphere 2: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere 3: dihydrogen peroxide; water / 20 °C 4: toluene / 2 h / |Reflux 5: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
1: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere 2: dihydrogen peroxide; water / 20 °C 3: toluene / 2 h / |Reflux 4: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
1: dihydrogen peroxide; water / 20 °C 2: toluene / 2 h / |Reflux 3: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
1: dihydrogen peroxide; water / 20 °C 2: toluene / 2 h / |Reflux 3: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
1: dihydrogen peroxide; water / 20 °C 2: toluene / 2 h / |Reflux 3: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
1: dihydrogen peroxide; water / 20 °C 2: toluene / 2 h / |Reflux 3: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
1: water-d2; aq. phosphate buffer / 20 °C / pH 8 2: toluene / 2 h / |Reflux 3: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
1: water-d2; aq. phosphate buffer / 20 °C / pH 8 2: toluene / 2 h / |Reflux 3: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
1: water-d2; aq. phosphate buffer / 20 °C / pH 8 2: toluene / 2 h / |Reflux 3: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / acetonitrile / 2 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
