2-溴乙基基苯硼酸频哪醇酯合成路线 （共 25 条）
反应条件
sodium hydroxide in ethanol soln. ethanethiol and NaOH in EtOH was added dropwise to soln. (2-bromomethylphenyl)boronic acid pinacol ester in EtOH and stirreed for 30 min at room temp.; solvent was evapd., residue was purified by column chromy. on silica (hexane:EtOAc 20:1);
参考文献
Cody, John; Dennisson, Jeanette; Gilmore, Joshua; VanDerveer, Donald G.; Henary, Maged M.; Gabrielli, Alan; Sherrill, C. David; Zhang, Yiyun; Pan, Chia-Pin; Burda, Clemens; Fahrni, Christoph J.
Inorganic Chemistry, 2003 , vol. 42, # 16 p. 4918 - 4929
反应条件
1: acetonitrile; ethanol / 12 h / 20 °C
2: dihydrogen peroxide / dimethyl sulfoxide / 20 °C
3: water / dimethyl sulfoxide / 20 °C
View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
tetrabutylammomium bromide; potassium carbonate; sodium hydroxide
T=110°C; 0.0833333 h; Microwave irradiationin air;
参考文献
Spencer, John; Baltus, Christine B.; Patel, Hiren; Press, Neil J.; Callear, Samantha K.; Male, Louise; Coles, Simon J.
ACS Combinatorial Science, 2011 , vol. 13, # 1 p. 24 - 31
反应条件
1: acetonitrile; ethanol / 12 h / 20 °C
2: dihydrogen peroxide / dimethyl sulfoxide / 20 °C
3: water / dimethyl sulfoxide / 20 °C
View Scheme
参考文献
Cao, Sheng; Christiansen, Robin; Peng, Xiaohua
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 9050 - 9058
反应条件
PS-NMM in tetrahydrofuran
T=150°C; 0.25 h; Microwave irradiationin air;
参考文献
Spencer, John; Baltus, Christine B.; Patel, Hiren; Press, Neil J.; Callear, Samantha K.; Male, Louise; Coles, Simon J.
ACS Combinatorial Science, 2011 , vol. 13, # 1 p. 24 - 31
