2-(2-苯基乙硫基)乙醇合成路线 (共 2 条)
反应条件
1: NaBO3*4H2O / acetic acid / 20 °C
2: methanesulfonyl chloride; triethylamine / CH2Cl2 / 20 °C
View Scheme
参考文献
Leblanc, Andre; Fosset, Laurent; Magnaud, Gilbert; Delmas, Gerard; Desgranges, Michel; et al.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 79, # 1,4 p. 141 - 146
反应条件
pyridine; thionyl chloride
a) 0 deg C, 30 min, b) 50 deg C, 1 h;
参考文献
Leblanc, Andre; Fosset, Laurent; Magnaud, Gilbert; Delmas, Gerard; Desgranges, Michel; et al.
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 79, # 1,4 p. 141 - 146