4,4,5,5-四甲基-2-(4-辛基苯基)-1,3,2-二噁硼烷合成路线 （共 3 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane
T=-78 - 20°C; Inert atmosphere;
参考文献
Zhu, Minliang; Luo, Hao; Wang, Liping; Guo, Yunlong; Zhang, Weifeng; Liu, Yunqi; Yu, Gui
Dyes and Pigments, 2013 , vol. 98, # 1 p. 17 - 24
反应条件
pyridine; N,N'-dimethyl-N,N'-propyleneurea; manganese; H7I2NiO3.5; bis(1,2-diphenylphosphino)benzene; 4,4'-di-tert-butyl-2,2'-dipyridyl
T=60°C; 16 h; Inert atmosphere;
参考文献
Everson, Daniel A.; Shrestha, Ruja; Weix, Daniel J.
Journal of the American Chemical Society, 2010 , vol. 132, # 3 p. 920 - 921
反应条件
1: 4-n-octyliodobenzene With n-butyllithium in tetrahydrofuran; hexanes
T=-78°C; 0.333333 h;
2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran; hexanes
T=20°C;
参考文献
POLYERA CORPORATION
Patent: WO2008/63609 A2, 2008 ;
Location in patent: Page/Page column 51 ;
