2-(叔丁基氨基)乙酸乙酯合成路线 （共 8 条）
反应条件
methyltrioxorhenium (VII) in benzene 48 h; Ambient temperature;
参考文献
Zhu, Zuolin; Espenson, James H.
Journal of the American Chemical Society, 1996 , vol. 118, # 41 p. 9901 - 9907
反应条件
in acetonitrile T=20°C; 4 h;
参考文献
Pospisil, Jiri; Potacek, Milan
Tetrahedron, 2007 , vol. 63, # 2 p. 337 - 346
反应条件
Ir(tetratolylporphyrinato)CH3 in dichloromethane T=-78 - 22°C; Inert atmosphere;
参考文献
Anding, Bernie J.; Woo, L. Keith
Organometallics, 2013 , vol. 32, # 9 p. 2599 - 2607
参考文献
Baret,P. et al.
Bulletin de la Societe Chimique de France, 1972 , p. 2493 - 2501
反应条件
sodium hydroxide 0.75 h; Heating;
参考文献
Gribble, Gordon W.; Hirth, Bradford H.
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 3 p. 719 - 726
反应条件
1: 82 percent / pyridine / 1 h / 20 °C 2: 87 percent / 10 percent aq. NaOH / 2 h / Heating View Scheme
参考文献
Petride, Horia
Revue Roumaine de Chimie, 1991 , vol. 36, # 9-10 p. 1113 - 1122
反应条件
(i) aq. NaOH, (ii) NaNO2, aq. HCl; Multistep reaction;
参考文献
Gribble, Gordon W.; Hirth, Bradford H.
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 3 p. 719 - 726
反应条件
1: 10percent aq. NaOH / 0.75 h / Heating
2: conc. aq. HCl, aq. NaNO2 / Ambient temperature
3: trifluoroacetic anhydride / ethyl acetate / 1 h / 0 °C
View Scheme
参考文献
Gribble, Gordon W.; Hirth, Bradford H.
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 3 p. 719 - 726
