1: With thionyl chloride in methanol T=20°C; Inert atmosphere; 2: With hydrogenchloride in water Inert atmosphere; 3: With ammonia; ammonium chloride in water Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Guijarro, David; Pablo, Oscar; Yus, Miguel
Journal of Organic Chemistry, 2010 , vol. 75, # 15 p. 5265 - 5270
boron trifluoride diethyl etherate; acetic acid; zinc 1.) toluene, -78 deg C, 2.) H2O, 40 deg C, 2 h, sonication; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, David S.; Gallagher, Peter T.; Lightfoot, Andrew P.; Moody, Christopher J.; Slawin, Alexandra M. Z.; Swann, Elizabeth
Tetrahedron, 1995 , vol. 51, # 42 p. 11473 - 11488
