2-三氧代-2,3-二氢吡啶并[2,3-d]嘧啶-4(1h)-酮合成路线 (共 14 条)
反应条件
sodium hydroxide; nickel
参考文献
Oakes et al.
Journal of the Chemical Society, 1956 , p. 1045,1053
反应条件
in polyethyleneglycol
T=140 - 150°C; 4 h;
参考文献
Nikpour, Farzad; Mozafari, Roya; Paibast, Touraj
Heterocycles, 2009 , vol. 78, # 6 p. 1569 - 1571
反应条件
1: POCl3
2: NH3
3: ethanol
View Scheme
参考文献
Oakes et al.
Journal of the Chemical Society, 1956 , p. 1045,1053
反应条件
1: aqueous KMnO4 / Erwaermen des Reaktionsprodukts mit wss. HCl
2: 210 °C
View Scheme
参考文献
Robins; Hitchings
Journal of the American Chemical Society, 1955 , vol. 77, p. 2256,2259
反应条件
1: NH3
2: ethanol
View Scheme
参考文献
Oakes et al.
Journal of the Chemical Society, 1956 , p. 1045,1053
反应条件
1: 190 °C
2: POCl3
3: aq. NaOH solution
4: H2O; NaHS
View Scheme
参考文献
Robins; Hitchings
Journal of the American Chemical Society, 1955 , vol. 77, p. 2256,2259
反应条件
lithium hydride in N,N-dimethyl-formamide
Ambient temperaturethe mixture stirred until homogeneous;
参考文献
Koscik; Kristian; Gonda; Dandarova
Collection of Czechoslovak Chemical Communications, 1983 , vol. 48, # 11 p. 3315 - 3328
反应条件
sodium hydrogensulfide; water
参考文献
Robins; Hitchings
Journal of the American Chemical Society, 1955 , vol. 77, p. 2256,2259
参考文献
Robins; Hitchings
Journal of the American Chemical Society, 1955 , vol. 77, p. 2256,2259
反应条件
1: water; H2S; NaHS
2: aqueous NaOH
View Scheme
参考文献
Robins; Hitchings
Journal of the American Chemical Society, 1955 , vol. 77, p. 2256,2259