1-苯基-2,3,4,9-四氢-1H-beta-咔啉合成路线 (共 50 条)
反应条件
trifluoroacetic acid in N,N-dimethyl-formamide 6 h; Heatingother solvent, other catalyst;
参考文献
Singh, Harjit; Sarin, Rakesh; Singh, Kamaljit
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 132 - 134
反应条件
acetate buffer; water; benzaldehyde
参考文献
Hahn et al.
Justus Liebigs Annalen der Chemie, 1935 , vol. 520, p. 107,115
反应条件
potassium permanganate in tetrahydrofuran T=-3 - 3°C; 2 h;
参考文献
Mokrosz, M.J.; Paluchowska, M.H.; Misztal, S.
Polish Journal of Chemistry, 1995 , vol. 69, # 2 p. 264 - 268
反应条件
potassium permanganate in tetrahydrofuran 2 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Mokrosz, M.J.; Paluchowska, M.H.; Misztal, S.
Polish Journal of Chemistry, 1995 , vol. 69, # 2 p. 264 - 268
反应条件
in benzene 2 h; Heating;
参考文献
Hulinska, Hana; Taufmann, Petr; Frycova, Hana; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 373 - 380
反应条件
in benzene 2 h; Heating;
参考文献
Hulinska, Hana; Taufmann, Petr; Frycova, Hana; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1988 , vol. 53, # 2 p. 373 - 380
反应条件
tetrabutylammomium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile
T=20°C; 2 h;
参考文献
Panarese, Joseph D.; Waters, Stephen P.
Organic Letters, 2010 , vol. 12, # 18 p. 4086 - 4089
反应条件
C21H21ClIrNO2 in tetrahydrofuran; 2,2,2-trifluoroethanol
20 h; Inert atmosphere;
参考文献
Wu, Jianjun; Talwar, Dinesh; Johnston, Steven; Yan, Ming; Xiao, Jianliang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., 2013 , vol. 125, # 27 p. 7121 - 7125,5
反应条件
potassium permanganate in tetrahydrofuran
2 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Mokrosz, M.J.; Paluchowska, M.H.; Misztal, S.
Polish Journal of Chemistry, 1995 , vol. 69, # 2 p. 264 - 268
反应条件
tetrabutylammomium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile
T=20°C; 2 h;
参考文献
Panarese, Joseph D.; Waters, Stephen P.
Organic Letters, 2010 , vol. 12, # 18 p. 4086 - 4089