N,N,N-triethylamine N-oxide; copper(l) chloride in 1,4-dioxane
T=50°C; 10 h;
参考文献
Suzuki, Shigeaki; Onishi, Takashi; Fujita, Yoshiji; Misawa, Hiromitsu; Otera, Junzo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3287 - 3288
N-ethylmorpholine N-oxide; lithium iodide in N,N-dimethyl-formamide
r.t., 1 h, 50 deg C, 4 h; Yields of byproduct given;
参考文献
Suzuki, Shigeaki; Onishi, Takashi; Fujita, Yoshiji; Misawa, Hiromitsu; Otera, Junzo
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3287 - 3288
1: 73 percent / p-TsOH*H2O / benzene / 6 h / 45 °C / in the dark
2: NaIO4 / methanol; H2O / 20 h / 20 °C
3: (MeO)3P / methanol / 48 h / 20 °C
4: 66 percent / active MnO2 / CHCl3 / 24 h / 20 °C
View Scheme
