反应条件
1: 1.) n-BuLi / 1.) THF, HMPA, hexane, -78 deg C, 1.5 h, 2.) 6 h
2: 5percent sodium amalgam, disodium hydrogen phosphate / methanol / 2 h / 0 °C
3: 91 percent / PBr3, pyridine / diethyl ether / 6 h / -5 °C
View Scheme
参考文献
Sato, Kikumasa; Inoue, Seiichi; Onishi, Akira; Uchida, Nobuhiko; Minowa, Nobuto
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 761 - 769
