1,4,4,6-四甲基-3H-嘧啶-2-硫酮合成路线 （共 11 条）
反应条件
hydrogenchloride T=100 - 110°C; 4 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1013 - 1018
反应条件
hydrogenchloride T=100 - 110°C; 2.5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1013 - 1018
反应条件
T=150 - 160°C; 3.5 h; other 1-substituted-4,4,6-trimethyl-1,4-dihydropyrimidine-2(3H)-thiones, var. solvents, additives, and reaction times; Product distributionMechanism;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 30, # 8 p. 740 - 743
反应条件
in water 4 h; Heating;
参考文献
Singh, Harjit; Singh, Paramjit; Deep, Kanwal
Tetrahedron, 1983 , vol. 39, # 9 p. 1655 - 1660
参考文献
Singh, Harjit; Singh, Paramjit
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1013 - 1018
反应条件
1: methanol / 30 h / Ambient temperature
2: tetrahydrofuran / 30 h / Ambient temperature
3: aq. NaOH / CH2Cl2
View Scheme
参考文献
Kim, Yong Hae; Lim, Byoung Uk
Tetrahedron Letters, 1991 , vol. 32, # 18 p. 2057 - 2060
反应条件
hydrogenchloride in methanol
Ambient temperature;
参考文献
Singh, Harjit; Singh, Paramjit
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1013 - 1018
参考文献
Willems; Vandenberghe
Ind. chim. belge Sonderband 31. Congr. int. Chim. ind. Luettich, 1958 , p. Bd. 2, S. 476, 479
Full Text Show Details
Zigeuner et al.
Monatshefte fuer Chemie, 1975 , vol. 106, p. 1219,1230
反应条件
exothermic reaction;
参考文献
Singh, Harjit; Singh, Paramjit
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1013 - 1018
反应条件
in water
4 h; Heating;
参考文献
Singh, Harjit; Singh, Paramjit; Deep, Kanwal
Tetrahedron, 1983 , vol. 39, # 9 p. 1655 - 1660
