2,2,2-三氯乙基苯甲酸酯合成路线 （共 4 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; triethylamine in N,N-dimethyl-formamide
T=90°C; 3.5 h; other reagent, temperature, reaction time; Product distribution;
参考文献
Hans, Jeremy J.; Driver, Russell W.; Burke, Steven D.
Journal of Organic Chemistry, 2000 , vol. 65, # 7 p. 2114 - 2121
反应条件
10 platinum on carbon; hydrogen; tri-n-butyl-tin hydride in N,N-dimethyl acetamide
T=25°C; P=760.051 Torr; 1 h; Reagent/catalyst; chemoselective reaction;
参考文献
Sawama, Yoshinari; Imanishi, Takahiro; Nakatani, Ryosuke; Fujiwara, Yuta; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2014 , vol. 70, # 30 p. 4540 - 4546
反应条件
4-(N,N-dimethlyamino)pyridine; tributylphosphine in N,N-dimethyl-formamide
T=100°C;
参考文献
Hans, Jeremy J.; Driver, Russell W.; Burke, Steven D.
Journal of Organic Chemistry, 2000 , vol. 65, # 7 p. 2114 - 2121
反应条件
sodium tetrahydroborate; selenium in N,N-dimethyl-formamide
T=40 - 50°C; 1 h;
参考文献
Huang, Zhi-Zhen; Zhou, Xun-Jun
Synthesis, 1989 , # 9 p. 693 - 694
