4-(甲基硫代)苯甲酸甲酯合成路线 （共 25 条）
反应条件
Rh((5-H-dibenzo[a,d]cyclohepten-5-yl)2N)(PPh3); methacrylic acid methyl ester in tetrahydrofuran T=-30 - 25°C; 4 h; chemoselective reaction;
参考文献
Zweifel, Theo; Naubron, Jean-Valere; Gruetzmacher, Hansjoerg
Angewandte Chemie - International Edition, 2009 , vol. 48, # 3 p. 559 - 563
反应条件
methanol; 1,1-dimethylpropan-1-ol; sodium hydride; anhydrous cobalt diacetate in tetrahydrofuran T=40°C; P=760 Torr; 71 h; Irradiation;
参考文献
Marchal, Joel; Bodiguel, Jacques; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1995 , vol. 60, # 26 p. 8336 - 8340
反应条件
tellurium; Bi(NO3)3·5H2O; 5 palladium on charcoal; oxygen in methanol T=60°C; P=760.051 Torr; 8 h;
参考文献
Powell, Adam B.; Stahl, Shannon S.
Organic Letters, 2013 , vol. 15, # 19 p. 5072 - 5075
反应条件
oxygen; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride in tetrahydrofuran T=25°C; P=760.051 Torr;
参考文献
Kiran, I. N. Chaithanya; Lalwani, Komal; Sudalai, Arumugam
RSC Advances, 2013 , vol. 3, # 6 p. 1695 - 1698
反应条件
1,1-dimethylpropan-1-ol; sodium hydride; anhydrous cobalt diacetate in tetrahydrofuran T=40°C; P=760 Torr; 71 h; Irradiation;
参考文献
Marchal, Joel; Bodiguel, Jacques; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1995 , vol. 60, # 26 p. 8336 - 8340
反应条件
1: methyl (4-nitrophenyl)carboxylate With caesium carbonate in dimethyl sulfoxide 2: (methylthio)trimethylsilane in dimethyl sulfoxide T=20°C; 16 h;
参考文献
Qiao, Qi; Dominique, Romyr; Sidduri, Achyutharao; Lou, Jianping; Goodnow, Robert A.
Synthetic Communications, 2010 , vol. 40, # 24 p. 3691 - 3698
反应条件
potassium carbonate in dimethyl sulfoxide T=90°C; 16 h; Inert atmosphereGreen chemistry;
参考文献
Ji, Yuan; Sweeney, Jessica; Zoglio, Jillian; Gorin, David J.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11606 - 11611
反应条件
palladium diacetate; triphenylphosphine; p-benozquinone T=20°C; P=760.051 Torr; 4 h;
参考文献
Yamamoto, Yoshihiko
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 2-3 p. 478 - 492
反应条件
NaY faujasite T=150°C; 26 h;
参考文献
Selva, Maurizio; Tundo, Pietro
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1464 - 1470
反应条件
in methanol T=0 - 5°C; methylthiodeazoniation; dimerization;
参考文献
Barbero, Margherita; Degani, Iacopo; Diulgheroff, Nicola; Dughera, Stefano; Fochi, Rita; Migliaccio, Mara
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5600 - 5608
