2,3-二氢-1H-茚-1,5-二醇合成路线 （共 13 条）
反应条件
sodium tetrahydroborate in methanol-d4
T=0°C; Inert atmosphere;
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C
2: acetonitrile-D3; water-d2 / |Photolysis
3: sodium tetrahydroborate / methanol-d4 / 0 °C / |Inert atmosphere
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: water / acetonitrile-D3 / |Photolysis
2: sodium tetrahydroborate / methanol-d4 / 0 °C / |Inert atmosphere
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: potassium permanganate / benzene / |Reflux; |Dean-Stark
2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C
3: acetonitrile-D3; water-d2 / |Photolysis
4: sodium tetrahydroborate / methanol-d4 / 0 °C / |Inert atmosphere
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C
2: acetonitrile-D3; water-d2 / |Photolysis
3: copper(ll) bromide / ethyl acetate; chloroform / |Reflux
4: silver(l) oxide / acetonitrile / 60 °C
5: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: water / acetonitrile-D3 / |Photolysis
2: copper(ll) bromide / ethyl acetate; chloroform / |Reflux
3: silver(l) oxide / acetonitrile / 60 °C
4: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: copper(ll) bromide / ethyl acetate; chloroform / |Reflux
2: silver(l) oxide / acetonitrile / 60 °C
3: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: potassium permanganate / benzene / |Reflux; |Dean-Stark
2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C
3: acetonitrile-D3; water-d2 / |Photolysis
4: copper(ll) bromide / ethyl acetate; chloroform / |Reflux
5: silver(l) oxide / acetonitrile / 60 °C
6: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: palladium 10 on activated carbon; hydrogen / ethyl acetate / 20 °C
2: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
反应条件
1: silver(l) oxide / acetonitrile / 60 °C
2: acetonitrile-D3; water-d2 / |Photolysis
View Scheme
参考文献
Kammath, Viju Balachandran; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Heger, Dominik; Klan, Petr; Rubina, Marina; Givens, Richard S.
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1718 - 1729
