1: 1-chloro-3-methoxy-benzene With magnesium in tetrahydrofuran
T=0°C; 2 h;
2: diethyl ((E)-4,8-dimethyl-3,7-nonadienyl)phosphonate in tetrahydrofuran
T=20°C; Further stages.;
参考文献
Ishihara; Ishibashi; Yamamoto
Journal of the American Chemical Society, 2001 , vol. 123, # 7 p. 1505 - 1506
1: CCl4, Ph3P / acetonitrile / 25 °C
2: diethyl ether; tetrahydrofuran; hexamethylphosphoric acid triamide / 6 h
View Scheme
参考文献
Nasipuri,D.; Chaudhuri,S.R.R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 262 - 265
in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether
6 h;
参考文献
Nasipuri,D.; Chaudhuri,S.R.R.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 262 - 265
