反应条件
1: PPh3; DEAD / tetrahydrofuran / 3 h / 20 °C
2: 93 mg / ammonium molybdate; aq. H2O2 / ethanol; tetrahydrofuran / 20 °C
3: 92 percent / LiHMDS / dimethylformamide; hexamethylphosphoric acid triamide; tetrahydrofuran / -35 - 20 °C
4: 98 percent / TBAF / tetrahydrofuran / 4 h / 20 °C
5: 87 percent / O2; NaHCO3 / Pt / H2O; acetone; propan-2-ol / 50 °C
View Scheme
参考文献
Liu; Jacobsen
Journal of the American Chemical Society, 2001 , vol. 123, # 43 p. 10772 - 10773
