4-N-(甲基磺酰胺)苯硼酸合成路线 (共 2 条)
反应条件
sodium hydrogencarbonate in water T=5 - 20°C; pH=7.2; 2 h; Cooling with ice;
参考文献
SANOFI; BELLEVERGUE, Patrice; GRAILHE, Patrick; MCCORT, Gary; O'CONNOR, Stephen; DUCLOS, Olivier
Patent: US2013/178472 A1, 2013 ;
Location in patent: Paragraph 0254 ;
反应条件
1: With pyridine in dichloromethane T=0 - 20°C; 2: With water in dichloromethane
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GMBH; BOEHRINGER INGELHEIM PHARMA GMBH and CO KG
Patent: WO2004/62663 A1, 2004 ;
Location in patent: Page/Page column 30 ;