8-甲氧基-9-硼杂双环[3.3.1]壬烷合成路线 (共 45 条)
反应条件
lithium aluminium tetrahydride isolation by trapping with 1-octene;;
参考文献
Gmelin Handbook: B: B-Verb.14, 5.6, page 212 - 224
反应条件
in tetrahydrofuran react. of dicyclohexylborane in THF with methoxyborane in hexanes at 0°C for 1-2 h, evapn.;
参考文献
Hoshi, Masayuki; Shirakawa, Kazuya; Arase, Akira
Chemical Communications, 1998 , # 11 p. 1225 - 1226
反应条件
in tetrahydrofuran react. of dicyclohexylborane in THF with methoxyborane in hexanes at 0°C for 2 h, evapn.;
参考文献
Hoshi, Masayuki; Shirakawa, Kazuya; Arase, Akira
Chemical Communications, 1998 , # 11 p. 1225 - 1226
反应条件
in tetrahydrofuran react. of dicyclohexylborane in THF with methoxyborane in hexanes at 0°C for 2 h, evapn.;
参考文献
Hoshi, Masayuki; Shirakawa, Kazuya; Arase, Akira
Chemical Communications, 1998 , # 11 p. 1225 - 1226
反应条件
in tetrahydrofuran react. of dicyclohexylborane in THF with methoxyborane in hexanes at 0°C for 2 h, evapn.;
参考文献
Hoshi, Masayuki; Shirakawa, Kazuya; Arase, Akira
Chemical Communications, 1998 , # 11 p. 1225 - 1226
反应条件
in tetrahydrofuran react. of dicyclohexylborane in THF with methoxyborane in hexanes at 0°C for 2 h, evapn.;
参考文献
Hoshi, Masayuki; Shirakawa, Kazuya; Arase, Akira
Chemical Communications, 1998 , # 11 p. 1225 - 1226
反应条件
in tetrahydrofuran react. of dicyclohexylborane in THF with methoxyborane in hexanes at 0°C for 2 h, evapn.;
参考文献
Hoshi, Masayuki; Shirakawa, Kazuya; Arase, Akira
Chemical Communications, 1998 , # 11 p. 1225 - 1226
反应条件
in tetrahydrofuran react. of dicyclohexylborane in THF with methoxyborane in hexanes at 0°C for 2 h, evapn.;
参考文献
Hoshi, Masayuki; Shirakawa, Kazuya; Arase, Akira
Chemical Communications, 1998 , # 11 p. 1225 - 1226
反应条件
in tetrahydrofuran react. of dicyclohexylborane in THF with methoxyborane in hexanes at 0°C for 2 h, evapn.;
参考文献
Hoshi, Masayuki; Shirakawa, Kazuya; Arase, Akira
Chemical Communications, 1998 , # 11 p. 1225 - 1226
反应条件
sodium hydroxide; dihydrogen peroxide; sodium methylate Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Imai, Toshiro; Perumal, P. Thirumali; Singaram, Bakthan
Journal of Organic Chemistry, 1985 , vol. 50, # 21 p. 4032 - 4036