2-三甲基硅氧基-1,3-丁二烯合成路线 （共 28 条）
反应条件
hydrogenchloride; hydroquinone; dihydroquinine
1) 150 deg C, 7 h, sealed tube, 2) reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Makin, S. M.; Shavrygina, O. A.; Nguyen, Fong Tung
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 11 p. 2082 - 2087
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 11 p. 2309 - 2315
反应条件
toluene-4-sulfonic acid
1.) reflux, 2.) benzene; Yield given. Multistep reaction;
参考文献
Skrydstrup; Audrain; Ulibarri; Grierson
Tetrahedron Letters, 1992 , vol. 33, # 32 p. 4563 - 4566
反应条件
toluene-4-sulfonic acid
1.) toluene, reflux, 36 h, 2.) benzene, reflux (Dean-Stark), 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Audrain, Helene; Skrydstrup, Troels; Ulibarri, Gerardo; Riche, Claude; Chiaroni, Angele; Grierson, David S.
Tetrahedron, 1994 , vol. 50, # 5 p. 1469 - 1502
反应条件
oxalic acid in trifluorormethanesulfonic acid; ethyl acetate; toluene; trifluoroacetic acid; benzene
参考文献
University of Melbourne
Patent: US4822873 A1, 1989 ;
反应条件
hydroquinone in toluene
45 h; Heating;
参考文献
Rigby, James H.; Kotnis, Atul; Kramer, James
Journal of Organic Chemistry, 1990 , vol. 55, # 17 p. 5078 - 5088
反应条件
in toluene
45 h; Heatingother dienophiles; Diels-Alder reaction, regioselectivity; Product distribution;
参考文献
Jung,M.E.; Mccombs,C.A.; Takeda,Y.
Journal of the American Chemical Society, 1981 , vol. 103, p. 6677
参考文献
Vice; De Carvalho; Taylor; Dmitrienko
Tetrahedron Letters, 1989 , vol. 30, # 52 p. 7289 - 7292
反应条件
hydrogenchloride; zinc(II) chloride
1.) acetonitrile, 4 h, 50 deg C; 2.) 10 min; Yield given. Multistep reaction;
参考文献
Vacca, J. P.
Tetrahedron Letters, 1985 , vol. 26, # 10 p. 1277 - 1280
