反应条件
1: 1.) dicyclohexylcarbodiimide, 4-dimethylaminopyridine / 1.) CH2Cl2, -5 deg C, 30 min, 2.) RT, 2 h 2: 70 percent / 740 - 760 °C / 0.02 Torr 3: N-bromosuccinimide / CCl4 / 1 h / Heating; Irradiation 4: 5percent NaOH / H2O / 100 °C 5: 95 percent / nickel peroxide, 2percent aq. NaOH / 18 h / Heating 6: trifluoroacetic anhydride / 1 h / Heating 7: 850 °C / 0.02 Torr View Scheme
参考文献
Anderson, Mark R.; Brown, Roger F. C.; Coulston, Karen J.; Eastwood, Frank W.; Ward, Annemarie
Australian Journal of Chemistry, 1990 , vol. 43, # 7 p. 1137 - 1150
