2-氨基-1-苯并[1,3]二氧代-5-乙酮盐酸盐合成路线 （共 3 条）
反应条件
hydrogenchloride; hydrogen; palladium on activated charcoal in methanol
P=2327.2 Torr; 5 h; Ambient temperature;
参考文献
Ackrell, Jack; Muchowski, Joseph M.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3374 - 3376
反应条件
1: 73 percent / sodium azide / dimethylsulfoxide / 25 °C
2: 81 percent / hydrogen / palladium on carbon / acetic acid / 25 °C / 760 Torr
View Scheme
参考文献
Giddens, Anna C.; Boshoff, Helena I.M.; Franzblau, Scott G.; Barry III, Clifton E.; Copp, Brent R.
Tetrahedron Letters, 2005 , vol. 46, # 43 p. 7355 - 7357
反应条件
1: 84 percent / p-TsOH*H2O; NBS / acetonitrile / Heating
2: 73 percent / sodium azide / dimethylsulfoxide / 25 °C
3: 81 percent / hydrogen / palladium on carbon / acetic acid / 25 °C / 760 Torr
View Scheme
参考文献
Giddens, Anna C.; Boshoff, Helena I.M.; Franzblau, Scott G.; Barry III, Clifton E.; Copp, Brent R.
Tetrahedron Letters, 2005 , vol. 46, # 43 p. 7355 - 7357
