反应条件
1.1: CH2Cl2 / 0 °C
2.1: H2 / 10 percent Pd/C / ethanol / 14 h / 20 °C / 760 Torr
3.1: Et3N; ClCO2Et / CH2Cl2 / 0.08 h / -10 °C
3.2: 75 percent / conc. ammonia / CH2Cl2 / 4 h
4.1: 64 percent / (CF3CO)2O; 1,8-diazabicyclo[5.4.0]undec-7-ene / dioxane / 1 h / 20 °C
5.1: 8 percent / AgF / CH2Cl2 / 20 h / 20 °C
View Scheme
参考文献
Bell, Stephanie E. V.; Brown, Roger F.C.; Eastwood, Frank W.; Horvath, Julianna M.
Australian Journal of Chemistry, 2000 , vol. 53, # 3 p. 183 - 190
