4,5-二溴噻吩-2-甲醛合成路线 (共 4 条)
反应条件
tetrahydro-4H-pyran; lithium diisopropyl amide T=-50°C;
参考文献
Froehlich, J.
Bulletin des Societes Chimiques Belges, 1996 , vol. 105, # 10-11 p. 615 - 634
反应条件
tetrafluoroboric acid; tri-tert-butyl phosphine; caesium carbonate; palladium diacetate in N,N-dimethyl-formamide T=90°C; Suzuki reaction; 12 h; Product distribution; Further Variations:ReagentsCatalystsSolvents;
参考文献
Handy, Scott T.; Mayi, Diyar
Tetrahedron Letters, 2007 , vol. 48, # 46 p. 8108 - 8110
反应条件
sodium tetrahydroborate; hydrogen; CaO; palladium in ethanol T=70°C; other solvents, other acceptor; Rate constant;
参考文献
Sharf, V. Z.; Belen'kii, L. I.; Gurovets, A. S.; Karmanova, I. B.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 2 p. 134 - 138
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 2 p. 176 - 180
反应条件
sodium tetrahydroborate; hydrogen; CaO; palladium in ethanol T=70°C; other solvents, other acceptor; Rate constant;
参考文献
Sharf, V. Z.; Belen'kii, L. I.; Gurovets, A. S.; Karmanova, I. B.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 2 p. 134 - 138
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 2 p. 176 - 180