双(2,4,5-三氯苯基)二硫化物合成路线 （共 14 条）
反应条件
toluene-4-sulfonic acid; triphenylphosphine in benzene 3 h; Heating;
参考文献
Oae; Togo
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 232 - 236
反应条件
1: 81 percent / chlorine, iodine / CCl4 2: tetramethylstannane / tetrakis(triphenylphosphine)palladium(0) / tetrahydrofuran / 4 h / 25 °C View Scheme
参考文献
Pilgram,K.; Korte,F.
Tetrahedron, 1965 , vol. 21, p. 1999 - 2013
反应条件
1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione; acetic acid in dichloromethane; water T=0 - 20°C; Inert atmosphere;
参考文献
Pu, Yu-Ming; Christesen, Alan; Ku, Yi-Yin
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 418 - 421
反应条件
1: (i) Cl2, (ii) /BRN= 956570/
2: 150 - 170 °C
3: aq. H2O2, AcOH, Ac2O
View Scheme
参考文献
Pilgram,K.; Korte,F.
Tetrahedron, 1965 , vol. 21, p. 1999 - 2013
