2-[(1,3-二氢-1,3-二氧代-2H-异吲哚-2-基)OXY]-4-甲基-丙酸-1,1-二甲基乙酯合成路线 （共 6 条）
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 3 h;
参考文献
Yang, Dan; Qu, Jin; Li, Wei; Wang, De-Ping; Ren, Yi; Wu, Yun-Dong
Journal of the American Chemical Society, 2003 , vol. 125, # 47 p. 14452 - 14457
反应条件
triphenylphosphine; diethylazodicarboxylate in tetrahydrofuran
参考文献
Yang; Li; Ng; Yan; Qu; Wu
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7303 - 7312
反应条件
1: aq. HCl; NaNO2 / 6 h / 0 °C
2: 4 h / 60 °C
3: DMAP; DCC / CH2Cl2 / 12 h / 20 °C
4: K2CO3 / methanol; H2O / 12 h / 20 °C
5: 70 percent / DEAD; PPh3 / tetrahydrofuran
View Scheme
参考文献
Yang; Li; Ng; Yan; Qu; Wu
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7303 - 7312
反应条件
1: 4 h / 60 °C
2: DMAP; DCC / CH2Cl2 / 12 h / 20 °C
3: K2CO3 / methanol; H2O / 12 h / 20 °C
4: 70 percent / DEAD; PPh3 / tetrahydrofuran
View Scheme
参考文献
Yang; Li; Ng; Yan; Qu; Wu
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7303 - 7312
反应条件
1: DMAP; DCC / CH2Cl2 / 12 h / 20 °C
2: K2CO3 / methanol; H2O / 12 h / 20 °C
3: 70 percent / DEAD; PPh3 / tetrahydrofuran
View Scheme
参考文献
Yang; Li; Ng; Yan; Qu; Wu
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7303 - 7312
反应条件
1: K2CO3 / methanol; H2O / 12 h / 20 °C
2: 70 percent / DEAD; PPh3 / tetrahydrofuran
View Scheme
参考文献
Yang; Li; Ng; Yan; Qu; Wu
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7303 - 7312
