in neat (no solvent)
byproducts: O2; transport reaction: passing F2-N2 mixture over KClO3 at 25 - 60°C;; washing with NaOH; passing ClO3F through Na2S2O3 soln.; drying over NaOH and P2O5;;
参考文献
Engelbrecht, A.; Atzwanger, H.
Journal of Inorganic and Nuclear Chemistry, 1956 , vol. 2, p. 348 - 357
Show Details
Gmelin Handbook: Cl: SVol.B2, 125, page 579 - 581
in neat (no solvent)
heating KClO3 and 98percent HSO3F at 85°C;; passing ClO3F through thiosulfate soln. and over solid KOH; condensation at temp. of liquid air;;
in neat (no solvent)
byproducts: O2; transport reaction: passing F2-N2 mixture over KClO3 at 25 - 60°C;; washing with NaOH; passing ClO3F through Na2S2O3 soln.; drying over NaOH and P2O5;;
参考文献
Engelbrecht, A.; Atzwanger, H.
Journal of Inorganic and Nuclear Chemistry, 1956 , vol. 2, p. 348 - 357
Show Details
Gmelin Handbook: Cl: SVol.B2, 125, page 579 - 581
