in acetic acid 0.0166667 h; Heating;

1: 5 percent / 3.3 N NaOCH3 / dimethylformamide; methanol / 1) -50 degC, 30 min, 2) -50 -> 0 degC 2: 73 percent / acetic acid / 0.02 h / Heating View Scheme

1: 94 percent / ethanol / 3 h 2: 5 percent / 3.3 N NaOCH3 / dimethylformamide; methanol / 1) -50 degC, 30 min, 2) -50 -> 0 degC 3: 73 percent / acetic acid / 0.02 h / Heating View Scheme

1: 85 percent / 1 N HCl / methanol / 5 h / Ambient temperature 2: 94 percent / ethanol / 3 h 3: 5 percent / 3.3 N NaOCH3 / dimethylformamide; methanol / 1) -50 degC, 30 min, 2) -50 -> 0 degC 4: 73 percent / acetic acid / 0.02 h / Heating View Scheme

1: 5 percent / 3.3 N NaOCH3 / dimethylformamide; methanol / 1) -50 degC, 30 min, 2) -50 -> 0 degC 2: 73 percent / acetic acid / 0.02 h / Heating View Scheme

1: 1) NaNO2 / 1) H2O, conc. HCl, 0 degC, 2) 2 N NaOH, -10 degC, 1 min 2: 85 percent / 1 N HCl / methanol / 5 h / Ambient temperature 3: 94 percent / ethanol / 3 h 4: 5 percent / 3.3 N NaOCH3 / dimethylformamide; methanol / 1) -50 degC, 30 min, 2) -50 -> 0 degC 5: 73 percent / acetic acid / 0.02 h / Heating View Scheme

hydrogen; Pd-BaSO4 in ethanol 0.166667 h;