反应条件
1.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / tetrahydrofuran / 30 °C / |Inert atmosphere 2.1: n-butyllithium / hexane; tetrahydrofuran / 0.75 h / -78 °C / |Inert atmosphere 2.2: 3 h / 0 - 20 °C / |Inert atmosphere 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / |Inert atmosphere 4.1: [Cp*Ru(CNCH3)3]+PF6- / methanol / 12 h / 90 °C / |Inert atmosphere View Scheme
参考文献
Garcia-Rubin, Silvia; Gonzalez-Rodriguez, Carlos; Garcia-Yebra, Cristina; Varela, Jesus A.; Esteruelas, Miguel A.; Saa, Carlos
Angewandte Chemie - International Edition, 2014 , vol. 53, # 7 p. 1841 - 1844
Angew. Chem., 2014 , vol. 53-126, # 7 p. 1872 - 1875